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  • Karl Fischer analysis for determining water content

    The trace moisture analyzer 초고압 전력을 사용하면 많은 전력 작업자가 다양한 전력 테스트를 더욱 편리하게 수행할 수 있습니다.

    HTY_2761

    Karl Fischer titration (KF) is a method in analytical chemistry that uses Coulombic, volumetric, or oven titration to determine trace levels of water content in a sample.   

    The Karl Fischer titration method is very popular because it has multiple practical advantages compared to other moisture determination methods, such as accuracy, speed, and selectivity. KF has selectivity towards water because the titration reaction itself consumes water. On the contrary, the measurement of quality loss during drying will detect the loss of any volatile substances. KF has high precision and accuracy, typically within 1% of available water, such as 3.00% displayed as 2.97-3.03%. KF response is linear and usually takes only a few minutes to complete. Therefore, using a calibrated 1% water standard for single point calibration is sufficient, and there is no need to calibrate the curve.

    Using KF requires almost no sample preparation. For volumetric and Coulombic methods, liquid samples can usually be directly injected into titration cups using a syringe. The main difference between the two is that using the volumetric method, the titrant is directly added to the sample through a burette, while using the Coulombic method, the titrant is generated electrochemically in the titration cell. For the oven method, the solid sample is sealed in a glass vial and then introduced into the oven, where the water content is pulled out and transferred to a Coulombic titration cell using a carrier funnel, where it is consumed and quantified.

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